Equipment database
- Name:
- Assembly for operando studies
- Producer:
- AXS, Hiden Analytical, IPC PAS, and others
- Model:
- unique apparatus
- Research group:
- Team 16. Structure of nanocrystals and their dynamics triggered by surface chemical reactions
- Description:
-
An assembly for studying the structure of powder materials by diffractometric methods with simultaneous analysis of the gas atmosphere during chemical reactions by mass spectrometry. Information is obtained about the crystallographic phases and chemical reactions in which they take part. The assembly is fully controlled by the distributed local network. The lab includes a sensitive X- ray diffractometer with a LynxEye belt counter (Bruker), a mass spectrometer (Hiden), a gas flow controllers (MKS), temperature controllers (Lumel, Omega), pressure measurement etc. The diffractometric analysis includes the possibility of recording subtle phase and surface changes of nanocrystalline materials. Temperature range - from -198oC to 550oC, pressure -10-2 Tr to 1 atm. Experiments completely programmed with the help of S.O. Linux scripts.
- Contact:
dr hab. Zbigniew Kaszkur
Research
- Type of measurement: Crystallite growth kinetics
- Test method: Monitoring the diffraction image as a function of temperature
Details
- Name of equipment: AXS, Hiden Analytical, IPC PAS, and others model: unique apparatus
- Type of measurement: Crystallite growth kinetics
- Test method: Monitoring the diffraction image as a function of temperature
- Cost of measurement from: 500 PLN
- Cost of measurement to: 2000 PLN
- User performing the measurement: dr hab. Zbigniew Kaszkur
| Parametr fizyczny | Wartość parametru od |
Wartość parametru do |
Opis parametru |
| Temperature | 75 K | 823 K | - |
| Atmospheric composition | - | - | He, O2, CO, NO, H2, N2 in any combination, purity 5.0 |
- Type of measurement: Phase transition kinetics
- Test method: Monitoring the composition of the camera's output gases and the evolution of the diffraction image
Details
- Name of equipment: AXS, Hiden Analytical, IPC PAS, and others model: unique apparatus
- Type of measurement: Phase transition kinetics
- Test method: Monitoring the composition of the camera's output gases and the evolution of the diffraction image
- User performing the measurement: dr hab. Zbigniew Kaszkur
| Parametr fizyczny | Wartość parametru od |
Wartość parametru do |
Opis parametru |
| Temperature | 75 K | 823 K | - |
| Atmospheric composition | - | - | He, O2, CO, NO, H2, N2 in any combination, purity 5.0 |